Surface Chemistry • Topic 2 of 3

Catalysis

A catalyst is a substance that changes the rate of a chemical reaction without itself being consumed in the overall change. It works by providing an alternative reaction path of lower activation energy. A catalyst does not alter the position of equilibrium or the value of $\Delta G$; it only helps the system reach equilibrium faster by speeding both the forward and the backward reaction equally. Substances that increase the activity of a catalyst are promoters (e.g. molybdenum in the Haber process), while those that destroy its activity are poisons (e.g. arsenic on the platinum catalyst in contact process).

Homogeneous catalysis. Here the catalyst is in the same phase as the reactants. Examples: oxidation of $\text{SO}_2$ to $\text{SO}_3$ by $\text{NO}$ in the lead-chamber process (all gases); hydrolysis of an ester catalysed by mineral acid (all in solution); inversion of cane sugar catalysed by $\text{H}^+$. In heterogeneous catalysis the catalyst is in a different phase from the reactants, usually a solid catalysing gaseous or liquid reactants. Examples: the Haber synthesis of $\text{NH}_3$ over finely divided iron; the contact process oxidation of $\text{SO}_2$ over $\text{V}_2\text{O}_5$; hydrogenation of vegetable oils over nickel; Ostwald oxidation of $\text{NH}_3$ over platinum gauze.

Adsorption theory of heterogeneous catalysis. The action of a solid catalyst is explained in five steps: (i) diffusion of reactant molecules to the catalyst surface; (ii) adsorption of reactant molecules on the surface; (iii) formation of an intermediate on the surface, weakening the bonds within the reactants; (iv) reaction of the adsorbed species to give the product; (v) desorption of the product, freeing the surface for fresh reactant. Adsorption increases the local concentration of reactants on the surface and lowers the activation energy, so the reaction speeds up. Old intermediate-compound ideas are special cases of this surface picture.

Features of solid catalysts. Two properties matter most. Activity is the ability to speed up a reaction; it depends on the strength of chemisorption — the gases must be adsorbed strongly enough to react but not so strongly that products cannot leave. For hydrogenation the catalytic activity falls roughly in the order $\text{Pt} > \text{Pd} > \text{Ni} > \text{Fe}$. Selectivity is the ability to steer a reaction towards a particular product. The same reactants can give different products on different catalysts; for example, carbon monoxide and hydrogen give methane over nickel, methanol over a $\text{Cu}/\text{ZnO}/\text{Cr}_2\text{O}_3$ catalyst, and a mixture of hydrocarbons over cobalt.

Shape-selective catalysis by zeolites. Zeolites are microporous aluminosilicates with a honeycomb of cavities and channels of molecular dimensions. They catalyse reactions selectively according to the size and shape of the reactant and product molecules, which must fit into the pores; this is called shape-selective catalysis. The well-known zeolite ZSM-5 converts alcohols directly into petrol (gasoline) by dehydrating them to a mixture of hydrocarbons. Zeolites are also used as cracking and isomerisation catalysts in the petroleum industry.

Enzyme catalysis. Enzymes are complex protein molecules produced by living cells that catalyse biochemical reactions; they are nature's catalysts. The reactant is the substrate. A small region of the enzyme, the active site, binds the substrate (lock-and-key fit), forms an enzyme-substrate complex, converts it to product and is then released. Characteristic features: enzymes are highly efficient (one molecule can transform millions of substrate molecules per minute), highly specific (each enzyme acts on a particular substrate, e.g. urease only on urea), work best at an optimum temperature (around $298$–$310\ \text{K}$) and an optimum pH ($5$–$7$), and their activity is increased by coenzymes/activators and decreased by inhibitors and poisons. Examples: maltase converts maltose to glucose; zymase converts glucose to ethanol; pepsin hydrolyses proteins.

Homogeneous versus heterogeneous catalysis
FeatureHomogeneous catalysisHeterogeneous catalysis
PhaseCatalyst and reactants in the same phaseCatalyst in a different phase (usually solid)
MechanismVia intermediate compounds in one phaseVia adsorption on the catalyst surface
SeparationHard to separate the catalystEasy to separate (filter the solid)
Example$\text{SO}_2 \to \text{SO}_3$ with $\text{NO}$ (lead-chamber); ester hydrolysis by acid$\text{N}_2+\text{H}_2\to\text{NH}_3$ over Fe; $\text{SO}_2\to\text{SO}_3$ over $\text{V}_2\text{O}_5$
1
Worked Example
Define a catalyst and state how it speeds up a reaction.
Solution
  1. A catalyst is a substance that changes the rate of a reaction without being consumed in the overall reaction.
  2. It provides an alternative path with lower activation energy.
  3. Lower activation energy means a larger fraction of molecules can react, so the rate rises.

Answer: A catalyst increases the rate by offering a path of lower activation energy without being used up.

2
Worked Example
Distinguish between homogeneous and heterogeneous catalysis with one example of each.
Solution
  1. Homogeneous catalysis: catalyst and reactants are in the same phase.
  2. Example: oxidation of $\text{SO}_2$ to $\text{SO}_3$ in presence of $\text{NO}$ gas (lead-chamber process), all gaseous.
  3. Heterogeneous catalysis: catalyst is in a different phase from the reactants.
  4. Example: synthesis of $\text{NH}_3$ from $\text{N}_2$ and $\text{H}_2$ over solid iron (Haber process).

Answer: Homogeneous = same phase (e.g. $\text{SO}_2$/$\text{NO}$); heterogeneous = different phase (e.g. Haber process over Fe).

3
Worked Example
Outline the steps of the adsorption theory of heterogeneous catalysis.
Solution
  1. Diffusion of reactant molecules to the catalyst surface.
  2. Adsorption of reactant molecules on the surface.
  3. Formation of an activated intermediate that weakens reactant bonds.
  4. Reaction of the adsorbed species to form products.
  5. Desorption of the products, freeing the surface for fresh reactant.

Answer: Diffusion, adsorption, intermediate formation, reaction, then desorption.

4
Worked Example
Why does the same mixture of CO and $\text{H}_2$ give different products on different catalysts?
Solution
  1. This illustrates the selectivity of solid catalysts.
  2. Over nickel, CO and $\text{H}_2$ give mainly methane.
  3. Over a $\text{Cu}/\text{ZnO}/\text{Cr}_2\text{O}_3$ catalyst they give methanol.
  4. Over cobalt they give a mixture of higher hydrocarbons.

Answer: Because catalysts are selective — each directs the reactants toward a particular product.

5
Worked Example
What is shape-selective catalysis? Name one zeolite and its industrial use.
Solution
  1. Shape-selective catalysis is catalysis in which the reaction depends on the size and shape of reactant and product molecules relative to the catalyst pores.
  2. Zeolites are microporous aluminosilicates with cavities of molecular dimensions, so only molecules of suitable size enter and react.
  3. The zeolite ZSM-5 converts alcohols into a mixture of hydrocarbons (petrol).

Answer: Catalysis governed by molecular size/shape fitting the pores; ZSM-5 converts alcohols to gasoline.

6
Worked Example
List three characteristics of enzyme catalysis.
Solution
  1. High efficiency: one enzyme molecule can transform a very large number of substrate molecules.
  2. High specificity: each enzyme acts on a particular substrate (e.g. urease only on urea).
  3. Optimum conditions: maximum activity at an optimum temperature (around body temperature) and optimum pH.

Answer: Enzymes are highly efficient, highly specific, and active only near an optimum temperature and pH.

Key Points

  • A catalyst speeds a reaction by lowering the activation energy and providing an alternative path; it does not change $\Delta G$ or the equilibrium position, only the rate.
  • Homogeneous catalysis has the catalyst in the same phase as the reactants (e.g. $\text{SO}_2$/$\text{NO}$); heterogeneous catalysis has it in a different phase (e.g. Fe in the Haber process).
  • Adsorption theory: reactants diffuse to the surface, are adsorbed, form an activated intermediate, react, and the products desorb — adsorption concentrates reactants and lowers $E_a$.
  • Solid catalysts are described by their activity (strength of adsorption, e.g. $\text{Pt}>\text{Pd}>\text{Ni}>\text{Fe}$ for hydrogenation) and selectivity (CO + $\text{H}_2$ give methane, methanol or hydrocarbons on different catalysts).
  • Zeolites give shape-selective catalysis (ZSM-5 converts alcohols to petrol); enzymes are protein catalysts that are highly efficient, highly specific and active at an optimum temperature and pH.
Tap an option to check your answer0 / 4
Q1.A catalyst increases the rate of a reaction by:
Explanation: A catalyst provides an alternative path of lower activation energy without altering $\Delta G$ or the equilibrium position.
Q2.Which is an example of heterogeneous catalysis?
Explanation: In the Haber process the solid iron catalyst is in a different phase from the gaseous reactants, so it is heterogeneous.
Q3.The ability of a catalyst to direct a reaction towards a particular product is called its:
Explanation: Selectivity is the ability of a catalyst to steer reactants toward one specific product; activity is its power to speed the reaction.
Q4.Which catalyst is used in the contact process for the oxidation of $\text{SO}_2$ to $\text{SO}_3$?
Explanation: Vanadium(V) oxide, $\text{V}_2\text{O}_5$, is the heterogeneous catalyst used in the contact process.